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焦耳热固定床反应器

PX-SYS-JHR

焦耳热直加热 · 同床双模对照 · 自研控制软件

产品介绍

一款面向快速热输入催化研究的新型固定床评价装置,控制软件与算法由谱迅自主研发。通过对夹持催化剂的导电碳毡或导电催化剂床层直接通电,使热量在反应区内部产生、实现秒级快速升温。装置集成可独立运行的焦耳热与电加热炉两种加热模式,便于在同一平台开展对照实验;标配四路气体、一路液体进料。适用于瞬态动力学、绿氢制备高温吸热催化、塑料与生物质热解等需要快速热输入或温度程序切换的催化研究。
焦耳热固定床反应器

产品优点

  • 秒级快速升温:热量在导电床层内部产生、缩短传热路径,升温响应快,适合瞬态动力学与快速催化筛选。
  • 同床双加热模式:集成焦耳热与独立电加热炉,同一床层不拆装即可对照内部发热与外部传导加热。
  • 隔离式贴壁测温:热电偶贴石英内衬管外壁、与加热回路电气隔离,避免电流干扰且无需穿刺床层。
  • 自研控制软件:谱迅自研 JouleReact 软件与控制算法,功率闭环 + 预测温度控制 + 装填自整定,自动适配不同催化剂、抑制过冲。
  • 多级安全 + 全程记录:软件多级安全联锁配合电源硬件过压/过流保护,运行数据逐秒记录。
  • 可拆换电极馈通:热区石墨电极,PTFE 绝缘衬管与 SS316 卡套布置于低温区,可重复拆装、耗材化。
  • 床层高度可调:催化剂床层高度可按装填量与实验需求调节。

产品参数

管道规格 英制 1/16、1/8,公制 3mm
催化剂装填量 0.1~10mL
压力范围 常压~10MPa(可定制 20MPa),控压精度 ±0.1MPa
进料系统 气体进料通道:4 个,BROOKS 5850E 质量流量控制器,量程及标定气体可定制;液体进料通道:1 个,选配液体柱塞泵,流量及设定范围可定制
气化预热炉 设计温度 700℃(可定制高温),精度 ±0.2℃,稳定性 ±0.2℃
反应炉(电加热炉) 设计温度 1000℃(可定制高温),精度 ±0.2℃,稳定性 ±0.2℃
加热方式 焦耳加热 + 电加热炉,双模式独立可控
焦耳热电源 可编程直流电源,4.8kW,0–60V,恒压/恒流可调,2U 全宽
加热载体 夹持催化剂的导电碳毡,或导电催化剂床层
加热电极 热区石墨电极,金属引线延伸至低温馈通区
电极馈通 PTFE 绝缘衬管 + SS316 卡套,低温区布置,可重复拆装、耗材化
测温方式 K 型铠装热电偶贴石英内衬管外壁、与加热回路电气隔离(间接贴壁测温)
焦耳热控制软件 谱迅自研 JouleReact 上位机软件与控制算法:功率闭环 + 预测温度 PID + 装填自整定 + 多级安全联锁 + 1s 数据记录
反应管 石英内衬管 + 316 不锈钢外管(石英内衬隔离催化剂与管壁);可定制 Inconel 用于超高温高压
控制与通讯 数字仪表 + 自研 JouleReact 软件,RS485 通讯,支持电脑远程控制与数据记录
选配部件 气液分离器、保温箱、加热带等
产品尺寸 可根据配置定制

Joule-Heating Fixed-Bed Reactor

PX-SYS-JHR

PRODUCT INTRO

A new fixed-bed catalyst-evaluation platform built around the Joule-heating effect, with in-house control software and algorithms. By passing current directly through the conductive carbon felt holding the catalyst, or through a conductive catalyst bed, Joule heat is generated inside the bed, achieving second-scale rapid heating and delivering heat directly into the reaction zone. It also integrates an independent electric-furnace mode that can run separately from or in comparison with the Joule-heating mode on the same reaction platform. It shares the multi-channel feed and control architecture of the tabletop/vertical fixed-bed reactors, with four gas channels and one liquid channel as standard. Suited to catalytic studies that require rapid heat input or temperature-program switching and are compatible with the electrode and reaction-tube materials, such as high-temperature endothermic catalysis in green-hydrogen production and pyrolysis of plastics and biomass.

PRODUCT ADVANTAGES

  • Second-scale rapid heating — Joule heat is generated inside the conductive bed, shortening the heat-transfer path for fast response; suited to transient kinetics and rapid catalyst screening
  • Same-bed dual heating modes — Joule heating and an independent electric furnace can heat the same bed, enabling comparison of internal vs. external heating without disassembly
  • Isolated non-intrusive wall-adjacent thermometry — the thermocouple sits against the outer wall of the quartz liner, electrically isolated from the powered bed, avoiding heating-current interference and without piercing the bed
  • In-house control software — the JouleReact software and control algorithms are developed in-house, with power closed-loop, predictive-temperature control and per-loading self-tuning that adapts to different catalysts and suppresses overshoot
  • Multi-level safety interlocks and full logging — software multi-level safety interlocks plus power-supply hardware over-voltage/over-current protection, with per-second CSV logging
  • Replaceable electrode feedthrough — graphite electrode in the hot zone, PTFE insulating liner and standard SS316 ferrule fitting in the low-temperature zone, allowing repeated disassembly and consumable replacement
  • Adjustable bed height — the catalyst bed height can be adjusted according to loading amount and experimental needs

PRODUCT SPECIFICATIONS

Tubing Spec Imperial 1/16, 1/8; metric 3 mm
Catalyst Loading 0.1–10 mL
Pressure Range Atmospheric–10 MPa (customizable to 20 MPa); pressure control accuracy ±0.1 MPa
Feed System Gas: 4 channels, BROOKS 5850E mass flow controllers, ranges and calibration gases customizable; Liquid: 1 channel, optional liquid plunger pump with customizable flow and range
Vaporization/Preheat Furnace Design temperature 700 °C (higher on request), accuracy ±0.2 °C, stability ±0.2 °C
Reaction Furnace (Electric-Furnace Mode) Design temperature 1000 °C (higher on request), accuracy ±0.2 °C, stability ±0.2 °C
Heating Method Joule heating + electric furnace, dual modes independently controllable
Joule-Heating Power Supply Programmable DC power supply, 4.8 kW, 0–60 V, constant-voltage/constant-current adjustable, 2U full-width
Heating Carrier Conductive carbon felt holding the catalyst, or a conductive catalyst bed energized directly
Heating Electrode Graphite electrode in the hot zone; metal lead extends to the low-temperature feedthrough zone
Electrode Feedthrough PTFE insulating liner + standard SS316 ferrule fitting, in the low-temperature zone, repeatedly detachable and consumable
Temperature Sensing Armored K-type thermocouple against the outer wall of the quartz liner, electrically isolated from the heating circuit (indirect wall-adjacent measurement)
Joule-Heating Control Software In-house JouleReact software and control algorithms: power closed-loop + predictive-temperature PID + per-loading self-tuning + multi-level safety interlocks + 1 s data logging
Reaction Tube Quartz liner + 316 stainless-steel outer tube (the quartz liner isolates the catalyst from the wall); Inconel available for ultra-high temperature and pressure
Control & Communication In-house JouleReact software + digital instrument, RS485 communication, remote PC control and data logging
Optional Components Gas-liquid separator, insulation box, heating tape, etc.
Dimensions Customizable per configuration