焦耳热固定床反应器
PX-SYS-JHR
焦耳热直加热 · 同床双模对照 · 自研控制软件
产品介绍

产品优点
- 秒级快速升温:热量在导电床层内部产生、缩短传热路径,升温响应快,适合瞬态动力学与快速催化筛选。
- 同床双加热模式:集成焦耳热与独立电加热炉,同一床层不拆装即可对照内部发热与外部传导加热。
- 隔离式贴壁测温:热电偶贴石英内衬管外壁、与加热回路电气隔离,避免电流干扰且无需穿刺床层。
- 自研控制软件:谱迅自研 JouleReact 软件与控制算法,功率闭环 + 预测温度控制 + 装填自整定,自动适配不同催化剂、抑制过冲。
- 多级安全 + 全程记录:软件多级安全联锁配合电源硬件过压/过流保护,运行数据逐秒记录。
- 可拆换电极馈通:热区石墨电极,PTFE 绝缘衬管与 SS316 卡套布置于低温区,可重复拆装、耗材化。
- 床层高度可调:催化剂床层高度可按装填量与实验需求调节。
产品参数
| 管道规格 | 英制 1/16、1/8,公制 3mm |
| 催化剂装填量 | 0.1~10mL |
| 压力范围 | 常压~10MPa(可定制 20MPa),控压精度 ±0.1MPa |
| 进料系统 | 气体进料通道:4 个,BROOKS 5850E 质量流量控制器,量程及标定气体可定制;液体进料通道:1 个,选配液体柱塞泵,流量及设定范围可定制 |
| 气化预热炉 | 设计温度 700℃(可定制高温),精度 ±0.2℃,稳定性 ±0.2℃ |
| 反应炉(电加热炉) | 设计温度 1000℃(可定制高温),精度 ±0.2℃,稳定性 ±0.2℃ |
| 加热方式 | 焦耳加热 + 电加热炉,双模式独立可控 |
| 焦耳热电源 | 可编程直流电源,4.8kW,0–60V,恒压/恒流可调,2U 全宽 |
| 加热载体 | 夹持催化剂的导电碳毡,或导电催化剂床层 |
| 加热电极 | 热区石墨电极,金属引线延伸至低温馈通区 |
| 电极馈通 | PTFE 绝缘衬管 + SS316 卡套,低温区布置,可重复拆装、耗材化 |
| 测温方式 | K 型铠装热电偶贴石英内衬管外壁、与加热回路电气隔离(间接贴壁测温) |
| 焦耳热控制软件 | 谱迅自研 JouleReact 上位机软件与控制算法:功率闭环 + 预测温度 PID + 装填自整定 + 多级安全联锁 + 1s 数据记录 |
| 反应管 | 石英内衬管 + 316 不锈钢外管(石英内衬隔离催化剂与管壁);可定制 Inconel 用于超高温高压 |
| 控制与通讯 | 数字仪表 + 自研 JouleReact 软件,RS485 通讯,支持电脑远程控制与数据记录 |
| 选配部件 | 气液分离器、保温箱、加热带等 |
| 产品尺寸 | 可根据配置定制 |
Joule-Heating Fixed-Bed Reactor
PX-SYS-JHR
PRODUCT INTRO
A new fixed-bed catalyst-evaluation platform built around the Joule-heating effect, with in-house control software and algorithms. By passing current directly through the conductive carbon felt holding the catalyst, or through a conductive catalyst bed, Joule heat is generated inside the bed, achieving second-scale rapid heating and delivering heat directly into the reaction zone. It also integrates an independent electric-furnace mode that can run separately from or in comparison with the Joule-heating mode on the same reaction platform. It shares the multi-channel feed and control architecture of the tabletop/vertical fixed-bed reactors, with four gas channels and one liquid channel as standard. Suited to catalytic studies that require rapid heat input or temperature-program switching and are compatible with the electrode and reaction-tube materials, such as high-temperature endothermic catalysis in green-hydrogen production and pyrolysis of plastics and biomass.
PRODUCT ADVANTAGES
- Second-scale rapid heating — Joule heat is generated inside the conductive bed, shortening the heat-transfer path for fast response; suited to transient kinetics and rapid catalyst screening
- Same-bed dual heating modes — Joule heating and an independent electric furnace can heat the same bed, enabling comparison of internal vs. external heating without disassembly
- Isolated non-intrusive wall-adjacent thermometry — the thermocouple sits against the outer wall of the quartz liner, electrically isolated from the powered bed, avoiding heating-current interference and without piercing the bed
- In-house control software — the JouleReact software and control algorithms are developed in-house, with power closed-loop, predictive-temperature control and per-loading self-tuning that adapts to different catalysts and suppresses overshoot
- Multi-level safety interlocks and full logging — software multi-level safety interlocks plus power-supply hardware over-voltage/over-current protection, with per-second CSV logging
- Replaceable electrode feedthrough — graphite electrode in the hot zone, PTFE insulating liner and standard SS316 ferrule fitting in the low-temperature zone, allowing repeated disassembly and consumable replacement
- Adjustable bed height — the catalyst bed height can be adjusted according to loading amount and experimental needs
PRODUCT SPECIFICATIONS
| Tubing Spec | Imperial 1/16, 1/8; metric 3 mm |
| Catalyst Loading | 0.1–10 mL |
| Pressure Range | Atmospheric–10 MPa (customizable to 20 MPa); pressure control accuracy ±0.1 MPa |
| Feed System | Gas: 4 channels, BROOKS 5850E mass flow controllers, ranges and calibration gases customizable; Liquid: 1 channel, optional liquid plunger pump with customizable flow and range |
| Vaporization/Preheat Furnace | Design temperature 700 °C (higher on request), accuracy ±0.2 °C, stability ±0.2 °C |
| Reaction Furnace (Electric-Furnace Mode) | Design temperature 1000 °C (higher on request), accuracy ±0.2 °C, stability ±0.2 °C |
| Heating Method | Joule heating + electric furnace, dual modes independently controllable |
| Joule-Heating Power Supply | Programmable DC power supply, 4.8 kW, 0–60 V, constant-voltage/constant-current adjustable, 2U full-width |
| Heating Carrier | Conductive carbon felt holding the catalyst, or a conductive catalyst bed energized directly |
| Heating Electrode | Graphite electrode in the hot zone; metal lead extends to the low-temperature feedthrough zone |
| Electrode Feedthrough | PTFE insulating liner + standard SS316 ferrule fitting, in the low-temperature zone, repeatedly detachable and consumable |
| Temperature Sensing | Armored K-type thermocouple against the outer wall of the quartz liner, electrically isolated from the heating circuit (indirect wall-adjacent measurement) |
| Joule-Heating Control Software | In-house JouleReact software and control algorithms: power closed-loop + predictive-temperature PID + per-loading self-tuning + multi-level safety interlocks + 1 s data logging |
| Reaction Tube | Quartz liner + 316 stainless-steel outer tube (the quartz liner isolates the catalyst from the wall); Inconel available for ultra-high temperature and pressure |
| Control & Communication | In-house JouleReact software + digital instrument, RS485 communication, remote PC control and data logging |
| Optional Components | Gas-liquid separator, insulation box, heating tape, etc. |
| Dimensions | Customizable per configuration |